Characterization of shale cores with low and anisotropic permeability is complicated, due to the presence of multiscale pore structure and thin layers, and defies conventional methods. To accurately reproduce the morphology of multiscale pore structure of the shale core, a novel core-scale reconstructing method is proposed to reconstruct 3D digital-experimental models by means of the combination of SEM, EDS images, nitrogen adsorption and pressure pulse decay experiment result. In this method, the multiscale and multicomponent reconstructing algorithm is introduced to build the representative multiscale model for each layer, which can describe the complex 3D structures of nano organic pores, micro-nano inorganic pores, micro slits and several typical minerals. Especially, to reproduce the realistic morphology for shale, the optimization algorithm based on simulated annealing algorithm uses the experimental data as constrain conditions to adjust and optimize the model for each layer. To describe the bedding characteristics of the shale core, bedding fractures are constructed by analysis of the mineral distribution in the interface of two layers, and then the representative models for different layers are integrated together to obtain the final core-scale digital-experimental model. Finally, the model is validated by computing its morphological and flow properties and comparing them with those of the actual 3D shale sample. This method provide a way for systematically and continuously describe the multiscale and anisotropic pore structure (from nm-cm) of the shale core, and will be helpful for understanding the quality of the shale reservoir.
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4.0 国际许可协议进行许可。
CSTR:11738.14.NCDC.XDA14.PP5621.2024
10.1038/s41598-019-39442-5